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FT/IR-4000 Series

ft-ir-4000-series1
The FT/IR-4000 series FTIR spectrometers has been designed to bring many of the features from the research grade FT/IR-6000 series into an affordable package for simpler applications such as QA/QC, materials identification and Academia.

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Features

The FT/IR-4600 is our entry level Mid-IR optical bench (7800 to 350 cm-1), but it still has a range of features that you find on research grade instruments, like KRS-5 windows to prevent damage to the interferometer. As standard It also has a Peltier stabilized DLA-TGS detector, as standard and a high output ceramic source. Optical alignment is guaranteed by corner cube (retro-reflective) mirrors with auto-alignment maximum energy throughput. With a resolution of 0.7cm-1 and a S/N greater than 25,000:1 this is more than entry level.

The FT/IR-4700 has all the same features as the FT/IR-4600 but has a higher resolution at 0.4cm-1 and a S/N at over 35,000:1, making it ideal for high resolution applications such as gas analysis.

For many routine sample analyses the FT/IR-4000 can be fitted with our new ATR-PRO ONE single bounce ATR with a choice of top plate material including a high throughput monolithic diamond, Germanium (ideal for carbon-black samples) and ZnSe. A choice of clamps with pressure up to 10,000 psi ensures good contact with the crystal.

The newly developed monolithic diamond provides excellent transmission and for the first time has great performance right down to 400cm-1

For flexible applications add a second detector such as an MCT or specify a different beamsplitter/detector combination to work in the Near-IR or Far-IR.

Couple the FT/IR-4000 optical bench to any of the FT-microscopes to create a system versatile to perform micro and macro FTIR spectroscopy.

With a simple USB connection to a PC -  Spectra Manager II software will run in XP/Vista to Windows 7 (32 and 64 bit) providing a customizable user interface for automating routine tasks such as sample identification and quality testing using Quick-Start and QC Compare (with build your own library capability).

KnowItAll informatics package is included, with 12,000 free spectra for life (250,000 for three months).

Based on over fifty years of experience in infrared spectroscopy and applying the most advanced technology, JASCO offers the best solutions for FT-IR analyses with a complete range of application-focused FT-IR spectrometers and sampling accessories as well as a dedicated instrument control and data analysis interface. The NEW FT/IR-4600 and 4700 FT-IR spectrometers provide a wide range of capabilities for education and routine analysis applications, featuring high quality, performance and reliability. They are also designed with flexibility and expandability in mind to meet with a wide range of expanding experimental requirements.

System Description

The most complete selection of FT-IR capabilitiesfrom education and routine analysis supplied with a standard automatic instrument validation system, providing instantaneous confirmation of instrument performance.

System Features

  • A full range of sampling accessories with IQ accessory recognition
  • Built-in auto-validation
  • Vibration-proof optical bench
  • Large sample compartment
  • Corner-cube (retro-reflective) mirrors with auto-alignment
  • Purgeable optics
  • Highly sensitive detector
  • Upgrade to include FTIR microscopy and IR Imaging
  • Rapid scan option
  • Wavenumber extension option
  • Optional 21-CFR-part 11 compliance
  • Vibrational Circular Dichroism (VCD) option

Simple and Easy-to-Use Operations

The FT/IR-4000 Series is controlled by JASCO's proprietary Spectra ManagerTM II cross-platform software. Spectra Manager has various functions such as spectra measurement, Quick-Start, spectral comparison and quantitative analysis as standard functions. The sample measurement screen can be customized according to user requirements and the customized screen and parameters can be saved for future use (User Adaptive Software capability). 

 

Advanced Measurement Screen of Spectra Manager II
Advanced Measurement Screen of Spectra Manager II

Sequence

Information such as the instrument status, measurement parameters and the sequence of data acquisition is displayed. 

Results display

Data analysis results such as spectral comparison and sample quantification are displayed and readily available. 

Real-time monitoring

A real-time data processing function can be used to verify the current spectrum during measurements. Spectra stored in thumbnails can also be overlaid with the current spectrum during sample measurements

Self-diagnosis

Self-diagnosis function allows verification of the current instrument status. 

Zoom

Target peak(s) and/or functional groups can be easily checked by a zoom function. 

Thumbnail

The measured spectra can be stored as thumbnails within the thumbnail window. 

The thumbnails can be individually selected and viewed in Spectra view. 

Real-time data processing

The data collection/processing sequence can be defined to include several data manipulation commands, activated as the spectral data is collected. The final result after all processing commands are completed are displayed as the final spectrum.

 

FT/IR-4000 Series Specifications

Model
FT/IR-4600
FT/IR-4700
Standard wavenumber measurement range 7,800 to 350 cm-1
Optional extended wavenumber range 15,000 to 2,200 cm-1, 5,000 to 220 cm-1
Display wavenumber range 15,000 to 0 cm-1 (standard)
Wavenumber accuracy Within ± 0.01 cm-1 (theoretical value)
Maximum resolution 0.7 cm-1 0.4 cm-1
Optical System Single beam
Sample chamber Size: 200 mm (W) × 260 mm (D) × 185 mm
Optical path: Center focus, light axis 70 mm high
Interferometer Configuration 45º Michelson interferometer
Corner cube mirror interferometer, with auto-alignment
mechanism, sealed structure, DSP control
Vacuum instrument -
Mirror coating Aluminum
Drive method Mechanical bearing, electromagnetic drive
Drive speed Auto, 1, 2, 3, 4 mm/sec
AUTO DLATGS 2.0 mm/sec
MCT (optional) 4.0 mm/sec
Rapid Scan 10 Hz (optional)
Beam splitter Substrate material Standard: Ge/KBr
Option: Si/CaF2, Ge/CsI (not interchangeable)
Replacement method -
Light source Standard: High-intensity ceramic source
Option: Halogen lamp (factory option only)
Detector DLATGS (with Peltier temperature control) (standard)
W-MCT, M-MCT, N-MCT, Si, InSb, InGaAs (optional)
Two detectors may be mounted simultaneously within the instrument.
Purging Interferometer, Sample compartment/Detector
Signal-to-noise ratio:
(4 cm-1, 1 min, near 2,200 cm-1)
25,000:1 35,000:1
Gain switching AUTO, 1, 2, 4, 8, 16, 32, 64, 128
100%T line flatness Within 100 ± 1.0%T
(4,000 to 700 cm-1, continuous repetitive measurement)
Communication USB 2.0
FTIR main unit Dimensions: 460 (W) × 645 (D) × 290 (H) mm
Weight:33 kg
Power supply unit Dimensions:200 (W) × 285 (D) × 90 (H) mm, Weight:4.7 kg
This unit can be placed on its base or on its side.

Standard Composition

Parts name Number Remarks
Power supply 1  
Connection cable 1 Cable for connecting the main unit to the power supply
AC cable 1 AC cable for the power supply
USB cable 1 Cable connecting the main unit to the PC
Sample holder 1  
Standard sample 1 Polystyrene film
Stepped pin 2 Used when installing optional accessories into the sample compartment.
Instruction manual 1  
Install Disk 1 Including Spectra ManagerTM II, QAU-4000
Quantitative program and KnowItAll JASCO Edition
Fuse 2  

* CFR Model does not include QAU-4000.
* LE or LE-CFR Models do not include QAU-4000 and KnowItAll JASCO Edition.

 

Details

 

FT/IR-4600

  • Maximum resolution: 0.7 cm-1
  • S/N ratio: 25,000:1
 

FT/IR-4700

  • Maximum resolution: 0.4 cm-1
  • S/N ratio: 35,000:1
 

Applications

Click one of the FTIR Spectroscopy applications below:

Evaluation of a Si Wafer Surface Using a 65-Degree Incident Angle ATR

Measurement of Oriented Films and Liquid Crystal Molecules by a Polarized ATR Accessory

Terahertz (THz) Measurements of Liquids by a Vacuum Compatible ATR Accessory

Rapid Identification of an Illegal Drug using NIR (Identification of MDMA Tablet)

Analysis Example by Vacuum Model FT/IR (2) Analysis of Low Concentration Gas

Secondary Structure Analysis of Proteins Using IR Imaging

Analysis of Automotive Fluids Using with FTIR

Pharmaceutical tablet characterization by NIR Imaging

Analysis Example by Vacuum Model FT/IR (1) Measurement of Silicon Wafer

Gas Analysis System using Full Vacuum Type FT/IR (Trace amount of H2O in N2 gas)

Quantitative Analysis of Powdered Solids with FTIR-ATR

Secondary Structure Analysis (SSE) Software for Infra Red Interpretation and Modeling of Proteins

Infrared Microscopy for the Analysis of Polymer Laminates in a Juice Bottle